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The material was then ground in a planetary ball mill (Retsch PM100) with four 40 mm diameter balls at 250 rpm for 2 h with counter-rotation occurring after 1 h to reduce the size of the large

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were subsequently wet milled down to sub-micron particle size with d 50=0.8 lm in a planetary ball mill (Fritsch Pulverisette 5) using zirconia grinding media of 3 mm (diameter =10 mm; height =5 mm) for sin-tering studies or toroids (outer diameter = 23 mm; inner diameter = 8 mm; height = 10 mm) for permeability measurements were prepared

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Grinding balls with diameter 3 mm and less must be weighed out. The above table provides you with the required mass per grinding bowl. The specified ball filling per bowl is the minimum quantity and should possibly be increased depending on the material properties.

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